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This system is an anti-corrosion manual sampling device. The parts in contact with the sampling medium are lined with PFA or Fluorine to achieve anti-corrosion purpose. The Teflon suction pipe matched with the insertion pipe (fluorine lined/ glass lined) is immersed below the medium liquid in the vessel to increase the stability of the process. The medium is sampled safely and quickly in the system by vacuuming.
安裝步驟:Installation procedure:
1.將(插入管)安裝到反應(yīng)釜相應(yīng)管口上緊固螺栓。
Install (the insertion pipe) on the corresponding nozzle of the reactor and fasten the bolts.
2.將取樣系統(tǒng)下端(底座)與(隔膜閥1)拆分,將(底座)安裝到(插入管)上端。
Separate the lower end (base) of the sampling system from (diaphragm valve 1), and install (base) to the upper end of (insertion pipe).
3.將四氟外翻邊(吸料管)裝入(底座)內(nèi)腔,四氟(吸料管)外翻邊處于(閥座)密封面處吻合。
Put the Teflon outer flanging (suction pipe) into the inner cavity of the (base), and the Teflon outer flange of (the suction pipe) is matched at the sealing surface of the (valve seat) .
4.將其余取樣系統(tǒng)主體與其連接緊固,保證(底座)密封處壓緊、無泄漏。
Connect and tighten the rest of the sampling system body to ensure that the sealing part of (base) is tight and without leakage.
備注:連接設(shè)備小口管徑時(shí)可取消底座部件。
Note: The base part can be canceled when connecting the device with small diameter pipe.
取樣步驟:
Sampling procedure
1.取樣前確認(rèn)、檢查:Confirm and check before starting:
a:所有隔膜閥處于關(guān)閉狀態(tài)。
All diaphragm valves are closed.
b:取樣系統(tǒng)內(nèi)、外無殘余物視鏡無破損。
There is no residue inside and outside the sampling system, and no damage to the sightglass.
c:真空系統(tǒng)與對應(yīng)真空接口相連并確保密封無泄漏。
The vacuum system is connected to the corresponding vacuum interface and ensure that the seal is leak-free.
d:反吹用0.2~0.3MPa氮?dú)鈿庠础?/span>
0.2~0.3 MPa nitrogen gas source is used for back blowing.
e:備用150/250mL硼硅玻璃取樣瓶1支。
One spare 150/250 ml borosilicate glass sampling bottle is needed.
2.吸料:Suction:
Remove the (sampling bottle) and seal the bottle mouth - put in (spare sampling bottle) 。
e:打開(隔膜閥1)——打開(隔膜閥5)——打開(隔膜閥3、隔膜閥4)。
Open (diaphragm valve 1)—Open (diaphragm valve 5)—Open (diaphragm valve 3 and diaphragm valve 4) .
a:打開(隔膜閥1)。
Open (diaphragm valve 1) .
b:適時(shí)打開(隔膜閥2)。
Open (diaphragm valve 2) in time.
c:觀察(視鏡)。浮球緩慢上升,充滿視鏡窗。
Observe (sightglass). The floater slowly rises and medium fills the sightglass window.
d:關(guān)閉(隔膜閥1、隔膜閥2)。
Close (diaphragm valve 1 and diaphragm valve 2) .
3.取樣:Sampling:
a:打開(隔膜閥3)。
Open (diaphragm valve 3)
b:打開(隔膜閥4)。觀察取樣瓶量劑。
Open (diaphragm valve 4). Observe the dosage of the sam-piing bottle.
c:關(guān)閉(隔膜閥3、隔膜閥4)。
Close (diaphragm valve 3 and diaphragm valve 4).
d:取下(取樣瓶)密封瓶口——裝入(備用取樣瓶)。
氮?dú)鈱⑾到y(tǒng)內(nèi)殘余物料反吹釜內(nèi)。
Make nitrogen blow the residual medium in the system back into the vessel.
f:關(guān)閉(隔膜閥1、隔膜閥3、隔膜閥4、隔膜閥5)。
Close (diaphragm valve 1、diaphragm valve 3、diaphragm valve 4 and diaphragm valve 5) .
g:取祥結(jié)束。
Sampling complete.
反應(yīng)釜帶手動取樣系統(tǒng)清洗過程說明: Descript ionoftheCleani ngProcessoftheReactorwithManua15amp|ingSystern:
在進(jìn)行整個(gè)反應(yīng)釜的清洗過程中, 可以按照以上取樣步驟描述進(jìn)行取樣系統(tǒng)內(nèi)部清洗、吹掃。
During the cleaning process of the whole reactor, the internal cleaning and purging of the sampling system can be carried out according to the above sampling steps.
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